Hints on maintenance of spectrometers with SRAR for metal analyses
There may be variations in one point or another for different types of spectrometer. The manufacturer should be asked to provide a complete maintenance list, which should be placed in a visible location in the direct vicinity of the spectrometer. A book should be kept in tabular form for maintenance jobs.
Daily
1. Check
argon supply; check argon flow rates
2. Check
vacuum readings
3. Test
power output meter
4.
Measure intensities of reference lines with a pure sample
5.
Recalibrate
6. Clean
spark stand at end of shift
Weekly
1.
Unscrew stand bottom plate and clean
2. Check
Ar analysis data protection
3.
Change printer ribbon
Monthly
1. Renew
electrode tip
2. Clean
Ar outlet
3.
Change oil or water in wash bottle
4. Check
oil level in vacuum pump
5. Clean
or change air filter mats
6. Test
cartridges for gas-cleaning the UV optics
Half-yearly
1.
Change oil in vacuum pump
2. Check
Ar purifier
3. Clean
instrument interior
Yearly
1.
General inspection by spectrometer manufacture’s Service Department
Other
maintenance:
1. During
the first few days after commissioning, the profile should be checked
frequently, and subsequently at longer intervals eg. monthly, for typical
analytical lines.
2. If
the intensities of the references fall below preset values the quartz windows
must be cleaned.
3.In
vacuum spectrometers ,if the switching times for the solenoid valve are too
short the pump must be operated on gas ballast. In so doing, the pump should
not be separated from the container.
4. Also
note maintenance instructions for sample preparation equipment.
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